HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-Chlorophenyl methyl sulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | o-Chlorothiophenol | HCID 80599 | — |
| Product | 2-Chlorophenyl methyl sulfide | HCID 2737363 | 89% |
Reaction Steps
2-Chlorothioanisole was prepared in 89% yield from commercially available 2-chlorothiophenol (4.0 g, 27.6 mmol) using methyl iodide (4.66 g, 32.81 mmol) according to the procedure described in preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686390B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-d3988462855f4d489543d79de4be0fd4 |
| Source note | uspto-grants-2004_02 |