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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2119711Generated: November 2, 2026

HCID 86586191, compound → HCID 86586192, compound

https://huagongshe.com/reaction/2119711

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86586191HCID 86586191—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86586192HCID 8658619271%

Reaction Steps

0.07 g of 6-t-butyl-5-hydroxy-4-(1-methyl-2-propenyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane synthesized in Example 12 was dissolved in 10 ml of ethanol and he solution was treated with 0.01 g of 10% palladium on carbon in the same manner as in Example 9 to give 0.05 g of 6-t-butyl-5-hydroxy-4-(1-methylpropyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane as a pale yellow oil (yield 71%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06686389B2
Source datasetuspto-grants-2004_02
ORD IDord-a06a5a1808664712b0f9cf3ba9c9437c
Source noteuspto-grants-2004_02