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HRID2119734

反应详情

EQUATION

反应方程式

HRID 2119734 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1
HCID31404

Butylated hydroxytoluene

C15H24O

结构：CCCC[Mg]CCCC
HCID178448196

未命名化合物

PRODUCTS

生成物

1
结构：[Mg+2].[O-]c1ccccc1.[O-]c1ccccc1
HCID13616137

Magnesium di(phenolate)

C12H10MgO2

AUXILIARIES

试剂、催化剂与溶剂

2
结构：C1CCCCC1
溶剂HCID8078

Cyclohexane

C6H12

结构：CCCCCCC
溶剂HCID8900

Heptane

C7H16

PROCEDURE

实验过程

0.637 g of 2,6-di-tert-butyl-4-methylphenol (from Aldrich) and 2.9 ml of a 1.0 molar solution of dibutylmagnesium (DBM) in heptane (from Aldrich) were combined at 25° C. and stirred for 10 hours in 26 ml of cyclohexane before use.

WORKUP

后处理

  1. customwere combined at 25° C.