HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-methylphenol → Magnesium di(phenolate)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-methylphenol | HCID 31404 | — |
| Reactant | HCID 178448196 | HCID 178448196 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | Magnesium di(phenolate) | HCID 13616137 | — |
Reaction Steps
0.637 g of 2,6-di-tert-butyl-4-methylphenol (from Aldrich) and 2.9 ml of a 1.0 molar solution of dibutylmagnesium (DBM) in heptane (from Aldrich) were combined at 25° C. and stirred for 10 hours in 26 ml of cyclohexane before use.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686423B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-7764d8546b2f43f0a50dc4efc0ff25fc |
| Source note | uspto-grants-2004_02 |