HRID2119748

反应详情

EQUATION

反应方程式

HRID 2119748 的结构方程式

PROCEDURE

实验过程

From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methyl-butyl)amide (precursor 5c) and phenyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 55 mg of 2′-(phenoxycarbonylaminomethyl)-biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as a resin. MS (ES+): m/e=417 (M+1).

WORKUP

后处理

  1. extractionfollowed by extraction with EA and purification by flash chromatography 55 mg of 2′-(phenoxycarbonylaminomethyl)-biphenyl-2-carboxylic acid (3-methylbutyl)amide
  2. customwere obtained as a resin