HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → 2'-(Phenoxycarbonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 2'-Aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide | HCID 67316109 | — |
| Product | 2'-(Phenoxycarbonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide | HCID 9931732 | — |
Reaction Steps
From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methyl-butyl)amide (precursor 5c) and phenyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 55 mg of 2′-(phenoxycarbonylaminomethyl)-biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as a resin. MS (ES+): m/e=417 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686395B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-64da57907a8a4e5dbfc21ccdc690e40f |
| Source note | uspto-grants-2004_02 |