HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylphenyl isothiocyanate → HCID 9878820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylphenyl isothiocyanate | HCID 29519 | — |
| Reactant | 1-Methyl-3-aminopyrazole | HCID 137254 | — |
| Product | HCID 9878820 | HCID 9878820 | 95% |
Reaction Steps
Prepared using Method A from 4.73 g (27.5 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 2.5 g (25.7 mmol) of 1-methyl-3-aminopyrazole to give 6.8 g of title compound as a white solid (95% yield, m.p. 217-218° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686476B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ed0cbf841fb348a7b7c654c420e18b88 |
| Source note | uspto-grants-2004_02 |