HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-(Azidomethyl)-5-methyl-1,2-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 3-(Bromomethyl)-5-methylisoxazole | HCID 2776304 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(Azidomethyl)-5-methyl-1,2-oxazole | HCID 23440937 | — |
Reaction Steps
To a solution of the 3-bromomethyl-5-methyl-isoxazole in acetone is added NaN3 at rt. The reaction mixture is then stirred for about 48 h. Then, the reaction mixture is poured into water and extracted with EtOAc, dried and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686352B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-d40a14bb0478455e98f221682ad6f4aa |
| Source note | uspto-grants-2004_02 |