HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 23440965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 1-(5-Methyl-1,2-oxazol-3-yl)methanamine | HCID 2776306 | — |
| Product | HCID 23440965 | HCID 23440965 | — |
Reaction Steps
A solution of the C-(5-methyl-isoxazol-3-yl)-methylamine (150 mg, 1.3 mmol) in N,N-dimethylformamide dimethylacetal (2 mL, 14.4 mmol) was heated under reflux for 3 h. After cooling to room temperature, the solvent was evaporated to leave the title compound as a yellow oil (220 mg, 98%. m/z 168.2 (MH)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686352B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-768b6cb3ca8f4ca1a9c26794e7249375 |
| Source note | uspto-grants-2004_02 |