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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2120109Generated: October 30, 2026

Potassium Carbonate → HCID 23438624, compound

https://huagongshe.com/reaction/2120109

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantN-methyl-2-pyrrolidoneHCID 13387—
Reactant2,5-DibromopyridineHCID 69353—
ProductHCID 23438624HCID 23438624—

Reaction Steps

In 100 ml of 1-methyl-2-pyrrolidone was dissolved 10 g of 2,5-dibromopyridine which was then added with 3.5 ml of 3-pyrrolidine, along with 8.7 g of potassium carbonate at room temperature, followed by reacting them at 100° C. for 24 hours. After completion of the reaction, the same post-treatment was carried out as in Preparation Example 3 to obtain the title compound. 8 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06689779B2
Source datasetuspto-grants-2004_02
ORD IDord-ced979dd02a145c296b21c82beee50c2
Source noteuspto-grants-2004_02