HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 23438624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | 2,5-Dibromopyridine | HCID 69353 | — |
| Product | HCID 23438624 | HCID 23438624 | — |
Reaction Steps
In 100 ml of 1-methyl-2-pyrrolidone was dissolved 10 g of 2,5-dibromopyridine which was then added with 3.5 ml of 3-pyrrolidine, along with 8.7 g of potassium carbonate at room temperature, followed by reacting them at 100° C. for 24 hours. After completion of the reaction, the same post-treatment was carried out as in Preparation Example 3 to obtain the title compound. 8 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689779B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ced979dd02a145c296b21c82beee50c2 |
| Source note | uspto-grants-2004_02 |