HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 23438670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1H-1,2,3-Triazole | HCID 67516 | — |
| Reactant | 2,5-Dibromopyridine | HCID 69353 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 23438670 | HCID 23438670 | — |
Reaction Steps
In 20 ml of 1-methyl-2-pyrrolidone was dissolved 1.72 g of 2,5-dibromopyridine, followed by the addition of 500 mg of 2H-(1,2,3)-triazole and 3 g of potassium carbonate at room temperature. Reaction was conducted at 100° C. for 24 hours. After completion of the reaction, the same post-treatment as in Preparation Example 3 was carried out to obtain the title compound. 120 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689779B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-1cee0ae877e8483c893d0e8ec057fb71 |
| Source note | uspto-grants-2004_02 |