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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2120110Generated: November 1, 2026

Potassium Carbonate → HCID 23438670, compound

https://huagongshe.com/reaction/2120110

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant1H-1,2,3-TriazoleHCID 67516—
Reactant2,5-DibromopyridineHCID 69353—
SolventN-methyl-2-pyrrolidoneHCID 13387—
ProductHCID 23438670HCID 23438670—

Reaction Steps

In 20 ml of 1-methyl-2-pyrrolidone was dissolved 1.72 g of 2,5-dibromopyridine, followed by the addition of 500 mg of 2H-(1,2,3)-triazole and 3 g of potassium carbonate at room temperature. Reaction was conducted at 100° C. for 24 hours. After completion of the reaction, the same post-treatment as in Preparation Example 3 was carried out to obtain the title compound. 120 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06689779B2
Source datasetuspto-grants-2004_02
ORD IDord-1cee0ae877e8483c893d0e8ec057fb71
Source noteuspto-grants-2004_02