HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-2-thiophenecarboxaldehyde → HCID 69927084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-2-thiophenecarboxaldehyde | HCID 61663 | — |
| Reactant | Methyl 5,6-diaminopyridine-3-carboxylate | HCID 9920476 | — |
| Reactant | O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine | HCID 11830845 | — |
| Product | HCID 69927084 | HCID 69927084 | — |
Reaction Steps
The title compound, MS m/e (%): 289.2 (M+, 100), was prepared in accordance with the general method of example 1 from 5,6-diamino-nicotinic acid methyl ester, O-mesitylene-sulfonylhydroxylamine, and 5-methylthiophene-2-carboxaldehyde. The purification was performed by flash column chromatography on silica eluting with a mixture of ethyl acetate and n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689790B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-17ee18579ccd4028b3b1247090d8f983 |
| Source note | uspto-grants-2004_02 |