HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 23438899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 12094546 | HCID 12094546 | — |
| Product | HCID 23438899 | HCID 23438899 | 82% |
Reaction Steps
47% hydrobromic acid solution (1.6 ml) was added to 3-[6-(3,4-dimethoxyphenyl)benzo[b]furan-3-yl]pyridine (80 mg, 0.2414 mmol) obtained in Example 10, and the mixture was refluxed for 12 hours. The precipitate was filtered to obtain a pale yellow powder of 4-[3-(3-pyridyl)benzo[b]furan-6-yl]-1,2- benzenediol hydrobromide (76 mg, 82%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689798B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-4e60e5717bc946e1bbad4c1052276324 |
| Source note | uspto-grants-2004_02 |