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3,5-Dichlorosalicylaldehyde → HCID 57096104、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dichlorosalicylaldehyde | HCID 66660 | — |
| 反応物 | HCID 54077377 | HCID 54077377 | — |
| 反応物 | Cyclopentanecarboxylic acid (2-oxo-2,3-dihydro-1H-indol-6-yl)-amide | HCID 54539339 | — |
| 生成物 | HCID 57096104 | HCID 57096104 | 40% |
反応手順
Cyclopentanecarboxylic acid (2-oxo-2,3-dihydro-1H-indol-6-yl)-amide was condensed with 3,5-dichlorosalicylaldehyde using method B to give a mixture of isomers of cyclopentanecarboxylic acid [3-(3,5-dichloro-2-hydroxy-benzylidene)-2-oxo-2,3-dihydro-1H-indol-6-yl]-amide as an orange solid which was reduced using method D to give 10 mg (40%) of cyclopentanecarboxylic acid [3-(3,5-dichloro-2-hydroxybenzyl)-2-oxo-2,3-dihydro-1H-indol-6-yl]-amide as an off-white crystalline solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06689806B1 |
| 出典データセット | uspto-grants-2004_02 |
| ORD ID | ord-0bec4b20e71b433ca039e7b530479732 |
| 出典メモ | uspto-grants-2004_02 |