Sulfuric Acid → HCID 9928747, compound

Participants

Reaction Steps

In a manner similar to Example 1(j), by reacting 0.4 ml of concentrated sulphuric acid in 5 ml of methanol with 860 mg (1.8 mmol) of 6-[3-(3-ethoxymethoxy-5-ethoxymethoxymethylbenzyloxy)phenyl]-2-methylheptan-2-ol in 5 ml of methanol and 5 ml of THF, after purification on a silica column (ethyl acetate 60-heptane 40), a colourless oil (m=510 mg. Y=79%) is obtained.

Provenance & Evidence