HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 57503375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 23439791 | HCID 23439791 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57503375 | HCID 57503375 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 1.25 ml of tetrabutylammonium fluoride with 250 mg (0.41 mmol) of 6-{3-[3,4-bis-(tert-butyldimethylsilanyloxymethyl)phenoxymethyl]phenyl}-2-methylheptan-2-ol in 7 ml of THF, after purification on a silica column (ethyl acetate 30-heptane 70), a colourless oil (m=130 mg; Y=85%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-1b0999968aa14bd385c4b0a579998cce |
| Source note | uspto-grants-2004_02 |