HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57241908, compound → HCID 9905506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57241908 | HCID 57241908 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 9905506 | HCID 9905506 | — |
Reaction Steps
414 mg (1.27 mmol) of 5-{2-[4-(5-hydroxy-5-methylhexyl)phenyl]vinyl}benzene-1,3-diol in 40 ml of dioxane and 42 mg of 10% palladium/carbon are placed in a reactor. A hydrogen pressure of 7 bar is exerted for 4 hours at room temperature. The reaction medium is filtered on celite and the filtrate is evaporated. The product is crystallized from an ethyl acetate/hexane mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ddd0acb08c374a04a6c2c5a222073fe2 |
| Source note | uspto-grants-2004_02 |