HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86759335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 69927359 | HCID 69927359 | — |
| Product | HCID 86759335 | HCID 86759335 | — |
Reaction Steps
In a manner similar to Example 8(k), by reacting 4.98 g (8.4 mmol) of 2-[6-(4-{2-[3-(tetrahydropyran-2-yl)-5-(tetrahydropyran-2-yloxy)phenyl]-vinyl}phenyl)-1,1-dimethylhexyloxy]tetrahydropyran with the solution of 100 ml of acetic acid, 50 ml of THF and 25 ml of water, whitish crystals (m=1.85 g; Y=65%) are obtained. m.p.=158-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-38b7d528b4554111a0ca71c770c78dad |
| Source note | uspto-grants-2004_02 |