Acetic Acid → HCID 54545894, compound

Participants

Reaction Steps

In a manner similar to Example 8(k), by reacting 2 g (4.3 mmol) of 2,2-dimethyl-7-(2-{4-[5-methyl-5-(tetrahydropyran-2-yloxy)hexyl]phenyl}vinyl-4H-benzo[1,3]dioxin in a solution of 50 ml of acetic acid+25 ml of THF+12.5 ml of water, after purification on a silica column (ethyl acetate 50-heptane 50), a white powder (m=44 mg; Y=3%) is obtained. m.p.=163-5° C.

Provenance & Evidence