HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 56991338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 69685427 | HCID 69685427 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 56991338 | HCID 56991338 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 402 mg (0.69 mmol) of 7-(3-{2-[3,5-bis(tert-butyldimethylsilanyloxy)phenyl]propenyl}phenyl)-2-methylheptan-2-ol with 1.4 ml of tetrabutylammonium fluoride 1M/THF, after purification on a silica column (ethyl acetate 40-heptane 60), white crystals (m=176 mg; Y=72%) are obtained. m.p. 113-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-3c98958ad196418588f89124bc6bc394 |
| Source note | uspto-grants-2004_02 |