HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 67278732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 69685730 | HCID 69685730 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67278732 | HCID 67278732 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 858 mg (1.47 mmol) of 6-(3-{2-[3,5-bis-(tert-butyldimethylsilanyloxymethyl)phenyl]vinyl}phenyl)-2-methylhexan-2-ol with 3.25 ml of tetrabutylammonium fluoride 1M/THF, after purification on a silica column (ethyl acetate), a white paste (m=460 mg; Y=88%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-c17a463bfb1c41c9bcf935a3c494b40b |
| Source note | uspto-grants-2004_02 |