HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 56997199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 57275873 | HCID 57275873 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 56997199 | HCID 56997199 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 207 mg (0.46 mmol) of 8-(3-{2-[3-(tert-butyldimethylsilanyloxy)phenyl]vinyl}phenyl)-2-methyloctan-2-ol with 0.5 ml of tetrabutylammonium fluoride 1M/THF, after purification on a silica column (ethyl acetate 30-heptane 70), a white powder (m=203 mg; Y=32%) is obtained. m.p.=142-3° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-75215a3de9454e259b43e97019ade51a |
| Source note | uspto-grants-2004_02 |