HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 57503378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 23439822 | HCID 23439822 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57503378 | HCID 57503378 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 250 mg (0.42 mmol) of 7-{3-[3,4-bis-(tert-butyldimethylsilanyloxymethyl)phenylethynyl]phenyl}-2-methylheptan-2-ol with 0.93 ml of tetrabutylammonium fluoride 1M/THF, after purification on a silica column (ethyl acetate 70-heptane 30), white crystals (m=132 mg; Y=86%) are obtained. m.p.=52-5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-4fec816dcb0347e9b8046246bd88716d |
| Source note | uspto-grants-2004_02 |