HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 57068259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 57166925 | HCID 57166925 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57068259 | HCID 57068259 | — |
Reaction Steps
In a manner similar to Example 1(j), by reacting 0.1 ml of concentrated sulphuric acid in 1 ml of methanol with 90 mg (0.2 mmol) of 5-{3-[2-(3,5-bis-ethoxymethoxyphenyl)vinyl]phenyl}pentan-1-ol in 1 ml of methanol and 1 ml of THF, after purification on a silica column (ethyl acetate 60-heptane 40), a white powder (m=33 mg; Y=55%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-d8662ed1193b41f086f35410acdcc491 |
| Source note | uspto-grants-2004_02 |