HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 67278647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 69686234 | HCID 69686234 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67278647 | HCID 67278647 | — |
Reaction Steps
In a manner similar to Example 1(j), by reacting 0.6 ml of concentrated sulphuric acid in 7.5 ml of methanol with 369 mg (0.65 mmol) of 2-{3-[2-(3,5-bis-ethoxymethoxyphenyl)vinyl}phenyl}-7-methyl-7-(tetrahydropyran-2-yloxy)octan-2-ol in 7.4 ml of THF, after purification on a silica column (ethyl acetate 70-heptane 30), a yellowish paste (m=220 mg; Y=92%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-18628a45159c4909ba4d0781474fb709 |
| Source note | uspto-grants-2004_02 |