HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium borohydride → HCID 69685513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium borohydride | HCID 4148881 | — |
| Reactant | HCID 69928039 | HCID 69928039 | — |
| Product | HCID 69685513 | HCID 69685513 | — |
Reaction Steps
In a manner similar to Example 53(e), by reacting 204 mg (0.46 mmol) of dimethyl 4-[3-((E)-7-hydroxy-1,7-dimethyloct-1-enyl)phenoxymethyl]-phthalate (prepared in a manner similar to Examples 72(a-c)) with 30 mg (1.4 mmol) of lithium borohydride, a colourless oil is obtained (m=146 mg; Y=82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-b8816c33e4da40b9a0523778177825f8 |
| Source note | uspto-grants-2004_02 |