Lithium borohydride → HCID 86759343, compound

Participants

Reaction Steps

In a manner similar to Example 53(e), by reacting 360 mg (0.8 mmol) of dimethyl 4-[3-((2E,4E)-6-hydroxy-1,1,6-trimethylhepta-2,4-dienyl)phenoxymethyl]phthalate (prepared from the previous product in a manner similar to Example 64(d)) with 70 mg (3.2 mmol) of lithium borohydride, a colourless oil is obtained (m=220 mg; Y=70%).

Provenance & Evidence