Hydrochloric Acid → HCID 21954458, compound

Participants

Reaction Steps

A mixture of 10 mmole of 1-(1-methacryloyloxy-1-methylethyl)-3,5-bis(2-methoxyethoxymethoxy)adamantane thus obtained, 1 mmole (in terms of HCl) of 6N-HCl and 40 ml of acetone was stirred at room temperature for 5 hours. The resulting reaction mixture was incorporated with an aqueous ammonium chloride solution, was extracted with ethyl acetate, the organic layer was concentrated, and the concentrate was subjected to column chromatography on a silica gel to thereby yield the title compound.

Provenance & Evidence