HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 86586428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | 3-Pyridineacetonitrile | HCID 80923 | — |
| Product | HCID 86586428 | HCID 86586428 | — |
Reaction Steps
3.00 g (25.4 mmol) of 3-pyridylacetonitrile and 4.23 g (25.4 mmol) tert-butoxybis(dimethylamino)methane were stirred at 100° C. for 2 h. In the course of this, liberated dimethylamine and t-butanol were led off to the atmosphere by a slight reduced pressure flow by means of a vacuum pump. After cooling, the deposited solid was filtered, washed with a little H2O and the title compound was thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06693102B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-757791d466b545f1a378b491ebf9d0c3 |
| Source note | uspto-grants-2004_02 |