Hydrochloric Acid → HCID 9924144, compound

Participants

Reaction Steps

To a solution of 6-13a (0.215 g, 0.580 mmol) in TBf/MeOH/H2O 3:1:1 (10 mL)) was added NaOH (1.16 mL of 1N solution in water, 1.16 mmol). After 30 minutes, the mixture was neutralized with HCl (1.16 mL of 1N solution in water, 1.16 mmol) and the solvents were evaporated. The residue chromatographed on silica gel (15% MeOH/CHCl3) to give 6-14a as a white solid.

Provenance & Evidence