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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2121361Generated: November 4, 2026

1-Phenylpiperazine → HCID 23433062, compound

https://huagongshe.com/reaction/2121361

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-PhenylpiperazineHCID 7096—
ReactantEthyl 6-chloronicotinateHCID 2799611—
ProductHCID 23433062HCID 23433062125.2%

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 3.72 g (0.02 mol) of ethyl 6-chloronicotinate and 6.44 g (0.04 mol) of N-phenylpiperazine was stirred at 100° C. for 1 hour. The reaction mixture was concentrated in vacuo. The residue was stirred with isopropanol. 7.8 g of a yellow solid were obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06696437B1
Source datasetuspto-grants-2004_02
ORD IDord-3cc143efec694cd5be7d9d8f26d10b01
Source noteuspto-grants-2004_02