反应详情

Thiophosgene (0.38 ml) is added to a two-phase mixture at room temperature of 4-((3-(1,1-dimethyl-ethyl)phenyl)oxy)-2,5-dimethylaniline (1.35 g) in toluene (6 ml) and sodium bicarbonate (840 mg) in water (6 ml). The reaction mixture obtained is stirred for 2 h and the phases are then separated by settling. The aqueous phase is extracted with toluene and the combined organic phases are then washed with water, dried (magnesium sulphate) and then concentrated to give the title product.

1. customThe reaction mixture obtained
2. customthe phases are then separated
3. extractionThe aqueous phase is extracted with toluene
4. washthe combined organic phases are then washed with water
5. dry with materialdried (magnesium sulphate)
6. concentrationconcentrated