HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 73855076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 73854985 | HCID 73854985 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 73855076 | HCID 73855076 | — |
Reaction Steps
The product of Example 192 was treated with boron tribromide in DCM at 25° C. After 15 min the product mixture was quenched with brine, concentrated and chromatographed (silica gel, 0-10% MeOH/DCM) to yield the title compound. MS(ESI): 540 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06696473B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ac9ae3b9f75c493fbd9be3ce0a104424 |
| Source note | uspto-grants-2004_02 |