HRID21350

反应详情

EQUATION

反应方程式

HRID 21350 的结构方程式

CONDITIONS

反应条件

温度
125 °C

PROCEDURE

实验过程

A five-liter three necked flask equipped with a thermometer, condenser, stirrer, and nitrogen inlet was charged with 2-isopropylaminoethylamine (2550 g, 25 moles) and urea (1500 g, 25 moles). The reaction mixture was heated to 125° C. for seven hours and then 170° C. until no more gas releasing was observed. About 3155 g of N-isopropyl-2-imidazolidone was obtained. The reaction is represented as follows: ##STR10##

WORKUP

后处理

  1. customA five-liter three necked flask equipped with a thermometer, condenser, stirrer, and nitrogen inlet
  2. custom170° C.