HuagongsheHuagongshe Chemistry Print Report · For research reference only
S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride → Dibenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride | HCID 131719016 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | Dibenzylamine | HCID 7656 | — |
Reaction Steps
S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride (prepared according to Example 15) was hydrolysed in aqueous ethanolic sodium hydroxide. The solvents were evaporated and the residue taken up in water and extracted 3 times with methylene dichloride. The extracts were dried (MgSO4), filtered and evaporated to give N-(3-mercaptopropy])dibenzylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05422355 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-dfd2f0be67984e6aabe343adb657573f |
| Source note | uspto-grants-1995_06 |