反应详情

S-[(N,N-dibenzyl)aminobutyl]isothiourea, hydrochloride (prepared according to Example 15) was hydrolysed in aqueous ethanolic sodium hydroxide. The solvents were evaporated and the residue taken up in water and extracted 3 times with methylene dichloride. The extracts were dried (MgSO4), filtered and evaporated to give N-(3-mercaptopropy])dibenzylamine.

1. customThe solvents were evaporated
2. extractionextracted 3 times with methylene dichloride
3. dry with materialThe extracts were dried (MgSO4)
4. filtrationfiltered
5. customevaporated