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HRID21429

反应详情

EQUATION

反应方程式

HRID 21429 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCc1ccc(-c2ccc(C(=O)O)cc2)cc1
HCID1714884

4-(4-octylphenyl)benzoic acid

C21H26O2

PRODUCTS

生成物

1
结构：CCCCCCCCc1ccc(-c2ccc(C(=O)Cl)cc2)cc1
HCID14745967

未命名化合物

PROCEDURE

实验过程

After 4'-n-octylbiphenyl-4-carboxylic acid (3.2 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4'-n-octylbiphenyl-4-carboxylic acid chloride.

WORKUP

后处理

  1. temperatureunder refluxing for 6 hours
  2. distillationunaltered thionyl chloride was distilled off