HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4'-Octyl-4-biphenylcarboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | AC55649 | HCID 1714884 | — |
| Product | 4'-Octyl-4-biphenylcarboxylic acid chloride | HCID 14745967 | — |
Reaction Steps
After 4'-n-octylbiphenyl-4-carboxylic acid (3.2 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours, unaltered thionyl chloride was distilled off to obtain 4'-n-octylbiphenyl-4-carboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05424005 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-5beec08eb29948b38b2aa6837fbf9204 |
| Source note | uspto-grants-1995_06 |