HRID21496

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)OC(=O)[C@@H]1CCCN1C(=O)[C@@H](CC1CCCCC1)NC(=O)OCc1ccccc1

HCID131719019

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)[C@@H]1CCCN1C(=O)[C@H](N)CC1CCCCC1

HCID131719018

未命名化合物

收率 100%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Z-DCha-Pro-OtBu (made by standard peptide coupling reactions) was hydrogenated in THF over 5% Pd-C at standard temperature and pressure for 24 h. Filtration and evaporation provided H-DCha-Pro-OtBu (oil, 100%).

WORKUP

后处理

filtrationFiltration and evaporation