HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 57269820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 10848352 | HCID 10848352 | — |
| Product | HCID 57269820 | HCID 57269820 | 45% |
Reaction Steps
Prepared from 5-methoxy-1-methyl-3-(methylthio)-1H-indole-2-carboxylic acid by the procedure of Example 1 with 40% aqueous methylamine solution substituted for ammonium hydroxide. Yield 45% after recrystallization from ethyl acetate-hexane; mp 137°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05424329 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-39659c9fe2714ece87712ca498ea8311 |
| Source note | uspto-grants-1995_06 |