HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 58006125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58006162 | HCID 58006162 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58006125 | HCID 58006125 | — |
Reaction Steps
A solution of Compound 101 (39 mg, 0.07 mmol) and trifluoroacetic acid (0.2 ml, 0.35 mmol) in dichloromethane (3 mL) was stirred at room temperature for 2 h. The product (Compound 102) was purified by basic alumina flash column chromatography using 3% MeOH and 97% CH2Cl2 solution as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08193203B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-1bc9de4b677d460da4086d9041e88904 |
| Source note | uspto-grants-2012_06 |