HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl isocyanate → HCID 58006224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl isocyanate | HCID 61277 | — |
| Reactant | HCID 58006120 | HCID 58006120 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58006224 | HCID 58006224 | — |
Reaction Steps
A solution of Compound 125 (15 mg, 0.03 mmol) and isopropyl isocyanate (2.8 mg, 0.03 mmol) in dichloromethane (2 mL) was stirred at room temperature for 1 h. The product (Compound 126) was purified by Neutral alumina Prep TLC plate using 10% MeOH and 90% CH2Cl2 solution as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08193203B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-827186e7302c4f6493c949470bae545c |
| Source note | uspto-grants-2012_06 |