HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → Ethyl 2-(2-iminopyridin-1(2H)-yl)acetate hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Product | Ethyl 2-(2-iminopyridin-1(2H)-yl)acetate hydrobromide | HCID 68699194 | — |
Reaction Steps
To 39 mL (0.35 mol) of ethyl bromoacetate is added 9.4 g (0.1 mol) of 2-aminopyridine portionwise at 0° C. The resulting mixture is allowed to warm to room temperature and stirred at this temperature for 30 minutes. The precipitate is collected and washed with hexane to give the desired compound as light tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08193214B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-139322c54df1428e9f9697ab542f9be2 |
| Source note | uspto-grants-2012_06 |