HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxyacetic Acid → HCID 22754110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxyacetic Acid | HCID 12251 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | 3-Amino-5-[(2-hydroxyethyl)carbamoyl]-2,4,6-triiodobenzoic acid | HCID 19777538 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 22754110 | HCID 22754110 | — |
Reaction Steps
Analogously to Example 1(c), 90.3 g. (150 mmol) of 5-amino-N-(2-hydroxyethyl)-2,4,6-triiodoisophthalamic acid and methoxyacetyl chloride, freshly prepared from 45.5 ml. of methoxyacetic acid/43.5 ml. of thionyl chloride, are reacted in dimethylacetamide; yield: 84.7 g. (84%) m.p. 285° C., with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04132731 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-9916acc7c5b64b7a93f3153c55054044 |
| Source note | uspto-grants-1979_01 |