HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adipoyl chloride → HCID 22754098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adipoyl chloride | HCID 61034 | — |
| Reactant | HCID 22754101 | HCID 22754101 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 22754098 | HCID 22754098 | — |
Reaction Steps
Analogously to Example 10, 5-amino-N-(2-hydroxy-1,1-dimethylethyl)-2,4,6-triiodoisophthalamic acid is reacted with hexanedioic acid dichloride in dimethylacetamide, and the reaction mixture is worked up. The thus-obtained product melts at 280°-281° C., with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04132731 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-67542e65236e4a7dab5358c725ec30a5 |
| Source note | uspto-grants-1979_01 |