HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 22754116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 22754101 | HCID 22754101 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 22754116 | HCID 22754116 | — |
Reaction Steps
Analogously to Example 3, 63.0 g. (100 mmol) of 5-amino-N-(2-hydroxy-1,1-dimethylethyl)-2,4,6-triiodoisophthalamic acid is reacted in 120 ml. of dimethylacetamide with 17 ml. of acetyl chloride and worked up. Yield: 64.0 g. (95%), m.p. 279°-281° C., with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04132731 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-09d9d98d66034d95826c634901d17133 |
| Source note | uspto-grants-1979_01 |