HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 22754119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 22754106 | HCID 22754106 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 22754119 | HCID 22754119 | 87% |
Reaction Steps
Analogously to Example 3, 5-amino-N-(2-hydroxypropyl)2,4,6-triiodoisophthalamic acid and acetyl chloride are reacted in dimethylacetamide. Yield: 87%, m.p. 276°-278° C., with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04132731 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-74a6df7704f74dff92fb48715cb35e35 |
| Source note | uspto-grants-1979_01 |