反应详情

0.2 mol (31.5 g) of 2-amino-4-chloroanisole, 40 ml of absolute alcohol, 20 ml of acetic anhydride and a pinch of zinc powder are placed in a 150 ml flask; the solution is brought to reflux for 30 minutes. The reaction liquid is poured onto crushed ice. The product obtained is separated; it is crystallized in a methanol/water mixture (20/80).

1. temperatureto reflux for 30 minutes
2. customThe reaction liquid
3. additionis poured
4. customonto crushed ice
5. customThe product obtained
6. customis separated
7. customit is crystallized in a methanol/water mixture (20/80)