HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 21333309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 21333313 | HCID 21333313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21333309 | HCID 21333309 | — |
Reaction Steps
Heat at reflux for 6 hours a mixture of 0.1 mole of cyanomethyl-5-(triphenylmethyl)-picolinate and 0.5 moles of diethylamine. Cool the reaction mixture, pour into water and extract with chloroform. Dry the chloroform layer over anhydrous sodium sulfate and evaporate to obtain thereby the product of this example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04133887 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-0aae57147389469f82a1e3c02086eb76 |
| Source note | uspto-grants-1979_01 |