HRID2163383

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6503

Tromethamine

C4H11NO3

结构：CCCc1c(OCC(O)COc2ccc3c(=O)cc(C(=O)O)oc3c2CCC)ccc(C(C)=O)c1O

HCID105007

未命名化合物

PRODUCTS

生成物

结构：CCCc1c(OCC(O)COc2ccc3c(=O)cc(C(=O)O)oc3c2CCC)ccc(C(C)=O)c1O.NC(CO)(CO)CO.O

HCID131711403

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

A solution of 0.121 parts of tris (hydroxymethyl) methylamine in 25 parts of ethyl alcohol was added to a solution of 0.498 parts of 7-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)-2-hydroxypropoxy]-4-oxo-8-propyl-4H-1-benzopyran-2-carboxylic acid in 25 parts of ethyl alcohol and the mixture heated on the steam bath for 5 minutes.

WORKUP

后处理

temperaturethe mixture heated on the steam bath for 5 minutes

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-0e596b54c57c4446a70c64efa0b37f06
来源数据集: uspto-grants-1979_01
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04133889
来源说明: uspto-grants-1979_01

反应 SMILES

[OH:1][CH2:2][C:3]([CH2:7][OH:8])([CH2:5][OH:6])[NH2:4].[C:9]([C:12]1[CH:40]=[CH:39][C:15]([O:16][CH2:17][CH:18]([OH:38])[CH2:19][O:20][C:21]2[CH:34]=[CH:33][C:24]3[C:25](=[O:32])[CH:26]=[C:27]([C:29]([OH:31])=[O:30])[O:28][C:23]=3[C:22]=2[CH2:35][CH2:36][CH3:37])=[C:14]([CH2:41][CH2:42][CH3:43])[C:13]=1[OH:44])(=[O:11])[CH3:10]>C(O)C>[OH2:1].[OH:1][CH2:2][C:3]([CH2:7][OH:8])([CH2:5][OH:6])[NH2:4].[C:9]([C:12]1[CH:40]=[CH:39][C:15]([O:16][CH2:17][CH:18]([OH:38])[CH2:19][O:20][C:21]2[CH:34]=[CH:33][C:24]3[C:25](=[O:32])[CH:26]=[C:27]([C:29]([OH:31])=[O:30])[O:28][C:23]=3[C:22]=2[CH2:35][CH2:36][CH3:37])=[C:14]([CH2:41][CH2:42][CH3:43])[C:13]=1[OH:44])(=[O:11])[CH3:10]